 
          3364
        
        
          Proceedings of the 18
        
        
          th
        
        
          International Conference on Soil Mechanics and Geotechnical Engineering, Paris 2013
        
        
          and coarse grained soils: coarse grained soils presents some
        
        
          structure alterations after freeze thaw cycles, fine grained soils
        
        
          presents heaves and changes of plasticity index due to water
        
        
          pulling during freezing. Most damages in road structures occur
        
        
          when subsoil on ground surface is made of fine grained soils
        
        
          (ZTVE-StB 94).
        
        
          Forages of vertical borehole heat exchangers attain depths in
        
        
          order of 100 m. Therefore, increasing of effective pressure with
        
        
          depth reduces the negative effects of freeze, as described by
        
        
          Ruckli (1950): for example, frost heave velocity for soils with a
        
        
          grain size between 0.005 mm and 0.010 mm decreases as
        
        
          pressure increases and is around equal to zero for pressures
        
        
          higher than 30 kN/m². Consequently, stress distribution in the
        
        
          soil and therefore on the borehole heat exchanger is considered
        
        
          as an important influence parameter. It leads to suppose that soil
        
        
          has a positive effect on frost resistance of the whole system,
        
        
          what should be verified here experimentally.
        
        
          3 ACTUAL STANDARDS AND TESTS
        
        
          There is actually no guideline for evaluating the frost resistance
        
        
          of vertical borehole heat exchangers. Developing a new
        
        
          procedure consists in defining the test experiments and the
        
        
          criteria regarding freezing resistance of the material. Following,
        
        
          an overview of the existing tests on freeze thaw resistance of
        
        
          different types of materials is given as base for possible
        
        
          procedures; under consideration that it should be further
        
        
          investigate with boundary conditions from vertical borehole
        
        
          heat exchangers.
        
        
          German and international standards for freeze-thaw
        
        
          experiments on soils exist for natural stones and aggregates. The
        
        
          German standard DIN 52104:1982 which gives instructions
        
        
          regarding freeze-thaw behavior of natural stones was replaced
        
        
          by the standard DIN EN 12371, from which the latest edition
        
        
          appeared in 2010. Details about the determination of the freeze
        
        
          thaw resistance of aggregates are given in the German standard
        
        
          DIN EN 1367-1.
        
        
          For unconsolidated material such as clay, silt and sand, there
        
        
          are no rules and standards. However, those types of soil are
        
        
          subject of research investigations (Rückli 1950, Simonsen and
        
        
          Isacsson 2001, Andersland and Ladanyi 2004).
        
        
          For freeze thaw resistance of hardened concrete according to
        
        
          the common standards, a distinction between freeze-thaw-
        
        
          resistance on the one hand with and on the other hand without
        
        
          de-icing agents is made (pre-standard DIN CEN/TS 12390-
        
        
          9:2006). The first one corresponds to the resistance to repeated
        
        
          freeze-thaw cycles in contact with water. In case of the second
        
        
          one, the specimen is in contact with road salt. Usually the de-
        
        
          icing agent corresponds to a 3% NaCl solution. In the pre-
        
        
          standard DIN CEN/TS 12390-9 three methods are described:
        
        
          the slab test as a reference, the cube method and the CF and
        
        
          CDF testing (Capillary Suction) as alternatives. The difference
        
        
          between CF and CDF method is the test fluid (with water or
        
        
          with deicing agent).
        
        
          Although no standards are available about freeze thaw
        
        
          resistance in application to borehole heat exchanger, some
        
        
          research reports deals specifically with freeze effects on grout
        
        
          materials (Herrmann 2008, Müller 2009, Niederbrucker et al.
        
        
          2008).
        
        
          Following test procedure takes care of those different
        
        
          standards and research reports and extends the actual analyses
        
        
          considering effects of freeze thaw with the surrounding soil.
        
        
          4 EXPERIMENTS AND RESULTS
        
        
          4.1
        
        
          
            Preliminary tests
          
        
        
          Experiments are conducted in a cylindrical encasement with a
        
        
          sample of grout material and soil. A more detailed description
        
        
          of the system for those tests is available in the next part.
        
        
          Preliminary tests has been conducted on samples with reduced
        
        
          dimensions in order to investigate the influence of water
        
        
          saturation of the surrounding soil and to validate the assembly
        
        
          procedure.
        
        
          Two samples of cement and sand are represented on figure 1.
        
        
          In both cases, cement characteristics and assembly procedure
        
        
          remains the same. If the surrounding soil has a low saturation
        
        
          degree, a cone appears on the upper part of the cement cylinder.
        
        
          The cement part possesses in this case higher unconfined
        
        
          compressive strength and modulus of elasticity with an
        
        
          increasing rate in the order of 40 %.
        
        
          Figure 1: Influence of the water saturation of the surrounding soil
        
        
          4.2
        
        
          
            Test procedure
          
        
        
          In order to avoid scaling factors, diameter of the grouting
        
        
          material cylinder is in the same range of diameters of real
        
        
          borehole heat exchangers, see figure 2 and 3. Dimensions of the
        
        
          cylindrical encasement were then selected taking in
        
        
          consideration the following statements: on one side, a large
        
        
          distance between rands of grouting material and rands of
        
        
          encasement limits the effects of deformations of the encasement
        
        
          on the grout material due to high temperature changes; on the
        
        
          other side, an increasing quantity of soil may lead to longer
        
        
          procedure time due to freezing and thawing periods and to more
        
        
          constraints regarding transport and storage due to an higher
        
        
          weight of the sample, which are to be considered for a
        
        
          reproductible procedure.
        
        
          Figure 2: Dimensions of the samples of soil and grouting material