 
          3377
        
        
          Technical Committee 307 + 212 /
        
        
          
            Comité technique 307 + 212
          
        
        
          3.2
        
        
          
            Data analysis
          
        
        
          For the needle probe, using Equations (3) and (4) for heating
        
        
          and recovery respectively, graphs were plotted of temperature
        
        
          against the natural logarithm of time, and the gradient of the
        
        
          straight line section used to determine the thermal conductivity.
        
        
          A typical result is shown in Figure 3.
        
        
          Figure 3. Graph of needle probe data for (a) heating and (b) recovery.
        
        
          For the thermal cell, average temperatures during the steady
        
        
          state period were calculated for each thermistor. The average
        
        
          power supplied to the cartridge heater was also calculated.
        
        
          Equation (5) was then used to determine the thermal
        
        
          conductivity.
        
        
          4 RESULTS AND DISCUSSION
        
        
          The results of the tests are shown in Table 1, with the average
        
        
          value of the five needle probe readings given. The needle probe
        
        
          consistently gave lower values of thermal conductivity than the
        
        
          thermal cell. The sample properties are given in Table 2, where
        
        
          the moisture content given is the average of the values before
        
        
          and after testing. There is a decrease in thermal conductivity
        
        
          with depth. This may be due to a decrease in density, and also
        
        
          change in mineralogy. The top two samples were of firm
        
        
          slightly sandy clay. The bottom sample had a significant
        
        
          number of fissures, and a slightly greater sand content.
        
        
          Table 1. Thermal conductivity measured using the needle probe for
        
        
          heating and recovery, and using the thermal cell.
        
        
          Thermal conductivity (Wm
        
        
          -1
        
        
          K
        
        
          -1
        
        
          )
        
        
          Sample depth
        
        
          (m)
        
        
          Needle probe
        
        
          in heating
        
        
          Needle probe
        
        
          in recovery
        
        
          Thermal cell
        
        
          8.00-8.45
        
        
          1.47
        
        
          1.30
        
        
          2.01 (t)*
        
        
          1.88 (b)
        
        
          10.00-10.45
        
        
          1.24
        
        
          1.36
        
        
          1.85 (t)
        
        
          1.91 (b)
        
        
          19.00-19.45
        
        
          1.06
        
        
          0.93
        
        
          1.65 (t)
        
        
          1.75 (b)
        
        
          *t – top half; b – bottom half.
        
        
          4.1
        
        
          
            Needle probe
          
        
        
          The variation in the five needle probe readings within the same
        
        
          sample was about ±10% for heating and ±15% for recovery.
        
        
          The sample at depth 19.00-19.45m had less variation. When the
        
        
          needle probe was previously tested using five identical agar gel
        
        
          samples, it gave a repeatability of ±2% for both heating and
        
        
          recovery, so most of the variation in results would seem to be
        
        
          due to natural variation in thermal conductivity of the soil.
        
        
          The greatest disadvantage with the needle probe is in the
        
        
          interpretation of results relying on human judgement. The
        
        
          calculated thermal conductivity is highly sensitive to the
        
        
          selection of the part of the graph deemed to be a straight line.
        
        
          Another factor which may affect the results is the use of contact
        
        
          fluid. In theory, the contact fluid should only decrease the time
        
        
          it takes to reach the straight line section of the graph, i.e. it
        
        
          should have no effect on the calculated thermal conductivity.
        
        
          However, the fluid could potentially seep into cracks in the soil,
        
        
          and in doing so alter the thermal conductivity. After testing, the
        
        
          specimens were cut up to see if this was the case. The soil at
        
        
          depths of 8.00-8.45m and 10.00-10.45m did not contain many
        
        
          fissures, and the contact fluid seemed to have stayed within the
        
        
          drilled holes. It can therefore be assumed that the contact fluid
        
        
          had little effect on the needle probe results. However, for the
        
        
          sample at depth 19.00-19.45m there were a significant number
        
        
          of fissures, which contact fluid had seeped into. This could
        
        
          affect both needle probe and thermal cell measurements, giving
        
        
          higher thermal conductivity results than otherwise.
        
        
          4.2
        
        
          
            Thermal cell
          
        
        
          In Section 2.2, two methods for calculating the thermal
        
        
          conductivity using the thermal cell were outlined. One involves
        
        
          measuring the power directly, the other uses the lumped
        
        
          capacitance method to calculate the power. Only the first
        
        
          method was deemed suitable for this study, as the temperature
        
        
          difference across the soil after the power is switched off was too
        
        
          great for lumped capacitance to apply i.e. Equation (6) was not
        
        
          satisfied.
        
        
          The difference in thermal conductivity values between the
        
        
          top and bottom sections was about 0.1Wm
        
        
          -1
        
        
          K
        
        
          -1
        
        
          . If the holes for
        
        
          the needle probe were to have a significant effect on the thermal
        
        
          conductivity values, the measurement for the top section would
        
        
          be expected to always be higher than for the bottom section, or
        
        
          vice versa. This is not the case, and as the area of the holes is
        
        
          only 1.25% of the total cross-sectional area, it can be assumed
        
        
          that the differences between the top and bottom sections are
        
        
          mainly due to the soil’s natural variability.
        
        
          The moisture content at the top of the specimens were
        
        
          measured before and after the thermal cell tests. The values
        
        
          after the test were consistently higher than those before the test.
        
        
          The greatest increase in moisture content was 5.2%. This shows
        
        
          that over the long heating period, moisture migration occurs in
        
        
          the direction of heat flow. This is where a temperature gradient
        
        
          causes the water to transfer latent heat through the pores as
        
        
          described by the liquid-island theory (Philip and de Vries,
        
        
          1957). This theory suggests that in fairly dry media, the water is
        
        
          deposited in isolated pockets or 'islands', either filling small
        
        
          pores or attaching themselves between soil grains. When a
        
        
          temperature gradient is applied, there is a vapour flux in the
        
        
          direction of heat flow. Water evaporates from one island, and
        
        
          condenses at the boundary of the next island, thereby
        
        
          transferring heat from one island to the next.
        
        
          4.3
        
        
          
            Comparing test methods
          
        
        
          The measured thermal conductivity for the thermal cell is higher
        
        
          than that of the needle probe by 40%, 45%, and 71% for a depth
        
        
          of 8.00-8.45m, 10.00-10.45m, and 19.00-19.45m respectively.
        
        
          This could be explained by a number of factors. The needle
        
        
          probe and thermal cell measure the thermal conductivity in the
        
        
          radial and axial directions respectively. It could be that the soil
        
        
          is anisotropic, and naturally has a higher thermal conductivity in
        
        
          the axial direction. However, the layers in the soil sample
        
        
          tended to be in the horizontal direction i.e. perpendicular to the
        
        
          cylinder axis. The thermal conductivity measured parallel to the
        
        
          layering should in general be higher than that measured
        
        
          perpendicular to the layering (Midttømme and Roaldset, 1998).
        
        
          If anisotropy was the reason behind the difference between
        
        
          needle probe and thermal cell values, then the needle probe
        
        
          would be expected to give higher values of thermal conductivity