 
          3376
        
        
          Proceedings of the 18
        
        
          th
        
        
          International Conference on Soil Mechanics and Geotechnical Engineering, Paris 2013
        
        
          Figure 1. TP02 probe (Hukseflux, 2003).
        
        
          2.2
        
        
          
            Thermal cell
          
        
        
          The thermal cell design was loosely based on Clarke et al.
        
        
          (2008). A diagram of the apparatus is shown in Figure 2. The
        
        
          thermal conductivity of a cylinder of soil is measured by
        
        
          generating one-directional heat flow along the axis of the
        
        
          specimen. The heat is generated by a cartridge heater embedded
        
        
          in the aluminium platen. Provided the specimen is well
        
        
          insulated so that radial heat losses can be neglected, the heat
        
        
          flow through the specimen during steady state is governed by
        
        
          Fourier’s Law of heat conduction:
        
        
          
            L
          
        
        
          
            TA Q
          
        
        
          
        
        
          
        
        
          
        
        
          (5)
        
        
          where
        
        
          
            Q
          
        
        
          is the power input,
        
        
          
            A
          
        
        
          is the cross-sectional area, Δ
        
        
          
            T
          
        
        
          is the temperature difference across the length of the specimen,
        
        
          and
        
        
          
            L
          
        
        
          is the length of the specimen. If
        
        
          
            Q
          
        
        
          cannot be accurately
        
        
          determined, measurement of the temperatures in the specimen
        
        
          as it cools after the power is switched off (the recovery phase)
        
        
          can be used to determine the heat transfer coefficient between
        
        
          the top of the soil and the air and hence the power. This uses the
        
        
          lumped capacitance method, which is valid when the
        
        
          temperature difference across the soil is small compared with
        
        
          the temperature difference between the soil surface and the
        
        
          ambient temperature (Incropera et al., 2007):
        
        
          1.0
        
        
          
        
        
          
        
        
          
        
        
          
            amb
          
        
        
          
            top
          
        
        
          
            top
          
        
        
          
            base
          
        
        
          
            T T
          
        
        
          
            T T
          
        
        
          (6)
        
        
          where subscripts
        
        
          
            base
          
        
        
          ,
        
        
          
            top
          
        
        
          and
        
        
          
            amb
          
        
        
          refer to temperature at
        
        
          the base of the soil, top of the soil, and of the ambient air
        
        
          respectively. Where this is satisfied, the temperature of the soil
        
        
          at time
        
        
          
            t
          
        
        
          is (Clarke et al., 2008):
        
        
          
        
        
          
        
        
          
        
        
          
        
        
          
        
        
          
        
        
          
        
        
          
        
        
          
        
        
          
        
        
          
        
        
            
        
        
          
            t
          
        
        
          
            mc
          
        
        
          
            hA
          
        
        
          
            T T TT
          
        
        
          
            p
          
        
        
          
            amb
          
        
        
          
            amb
          
        
        
          exp
        
        
          0
        
        
          (7)
        
        
          where
        
        
          
            T
          
        
        
          0
        
        
          is the temperature of the soil at time
        
        
          
            t
          
        
        
          = 0 (when
        
        
          Equation (6) starts to apply),
        
        
          
            h
          
        
        
          is the convection heat transfer
        
        
          coefficient,
        
        
          
            m
          
        
        
          is the total mass of the soil, and
        
        
          
            c
          
        
        
          
            p
          
        
        
          is the soil
        
        
          specific heat capacity. This is estimated from the properties of
        
        
          the soil constituents:
        
        
          
        
        
          
        
        
          
        
        
          
        
        
          
            water
          
        
        
          
            p
          
        
        
          
            soil
          
        
        
          
            p
          
        
        
          
            p
          
        
        
          
            mc
          
        
        
          
            mc
          
        
        
          
            mc
          
        
        
          
        
        
          
        
        
          (8)
        
        
          Equation (7) gives a theoretical decay curve which can be
        
        
          fitted to the experimental data by changing
        
        
          
            h
          
        
        
          until the two
        
        
          curves match. During steady state, conservation of energy
        
        
          dictates that the heat flow rate across the soil is equal to the heat
        
        
          flow rate at the top of the specimen from the soil to the air.
        
        
          
        
        
          
        
        
          
        
        
          
            amb
          
        
        
          
            top
          
        
        
          
            top
          
        
        
          
            base
          
        
        
          
            T ThA
          
        
        
          
            L
          
        
        
          
            T T
          
        
        
          
            A Q
          
        
        
          
        
        
          
        
        
          
        
        
          
        
        
          
        
        
          
        
        
          (9)
        
        
          This is used to calculate the thermal conductivity. It is worth
        
        
          noting that this method introduces an error associated with the
        
        
          estimation of the specific heat capacity from constituents whose
        
        
          properties may not be accurately known.
        
        
          Figure 2. Thermal cell.
        
        
          3 METHODOLOGY
        
        
          3.1
        
        
          
            Measurement procedure
          
        
        
          The thermal conductivity of U100 samples of London Clay
        
        
          taken from a thermal response test borehole were tested using
        
        
          both techniques described in Section 2. Before any
        
        
          measurements were taken, the sealed samples were left in a
        
        
          temperature controlled room overnight to equilibrate. Each
        
        
          sample was treated as follows.
        
        
          To accommodate the needle probe, a 200mm length
        
        
          specimen was prepared and secured in a rubber membrane.
        
        
          Shavings taken from the top of the sample were used to
        
        
          determine the initial moisture content at the top. The soil was
        
        
          found to be too hard to directly insert the probe. Therefore, a
        
        
          5mm diameter hole had to be predrilled, and the hole filled with
        
        
          a high thermal conductivity contact fluid (in this case toothpaste
        
        
          was used) to reduce the contact resistance between the probe
        
        
          and the soil (Hukseflux, 2003). The probe was inserted into the
        
        
          hole, and secured with a clamp stand. It was then left for 20min
        
        
          to equilibrate with the soil. A constant power was then supplied
        
        
          to the needle probe heater for 300s, and then turned off. The
        
        
          temperatures during the heating and recovery periods were
        
        
          recorded. Using this procedure, five measurements were taken
        
        
          over the cross-sectional area of the specimen. One measurement
        
        
          was taken at the centre of the cross-section, the other four were
        
        
          equally spaced at a radial distance of 25mm from the centre.
        
        
          To reduce the time it takes to reach steady state, the
        
        
          specimen was then cut in half and the top 100mm weighed and
        
        
          secured to the platen of the thermal cell (see Figure 2), and
        
        
          sealed at the top using aluminium foil to prevent moisture from
        
        
          leaving the top of the sample. Shavings taken from the bottom
        
        
          of the top half were used to determine the initial moisture
        
        
          content at the bottom. Insulation was then wrapped around the
        
        
          specimen. The temperature difference across the specimen is
        
        
          measured by two thermistors, one secured to the top of the
        
        
          platen, the other embedded at the top of the soil. The cartridge
        
        
          heater was then turned on, and the power controlled so that the
        
        
          platen remains at a constant temperature of 40°C. The power
        
        
          was measured using a MuRata ACM20-5-AC1-R-C wattmeter.
        
        
          Temperatures were monitored until steady state was reached
        
        
          and then maintained for at least 2hours. The power to the
        
        
          cartridge heater was then switched off, and the recovery period
        
        
          monitored. At the end of the test, shavings were taken from the
        
        
          top, middle and bottom of the specimen to determine the final
        
        
          moisture contents.
        
        
          The holes drilled into the specimen and the contact fluid
        
        
          could potentially affect the thermal conductivity measurement
        
        
          using the thermal cell. To verify the result, the bottom half of
        
        
          the sample was also tested in the thermal cell, where these
        
        
          effects would be less significant.
        
        
          A full soil classification was then conducted based on the
        
        
          British Standard 1377 (British Standards Institution, 1990), to
        
        
          determine the soil density, moisture content, liquid limit, plastic
        
        
          limit, particle density, and particle size distribution.