 
          1200
        
        
          Proceedings of the 18
        
        
          th
        
        
          International Conference on Soil Mechanics and Geotechnical Engineering, Paris 2013
        
        
          electrode resistivity systems (e.g. Damasceno et al., 2009) has
        
        
          triggered rapid and efficient data acquisition of resistivity
        
        
          measurements to address a wide range of applications such as
        
        
          water content estimations.
        
        
          A number of authors have demonstrated an explicit
        
        
          relationship between resistivity and water content. Shah and
        
        
          Singh (2005) proposed 'a generalized Archie's Law' as:
        
        
          m
        
        
          w
        
        
          
        
        
           
        
        
          
        
        
          
        
        
          (2)
        
        
          Where
        
        
          θ
        
        
          is the soil water content (volumetric),
        
        
          w
        
        
          
        
        
          is a fitting
        
        
          parameter related to pore water resistivity, and
        
        
          m
        
        
          is a
        
        
          dimensionless constant.
        
        
          2.2
        
        
          The multi-electrode resistivity system
        
        
          A multi-electrode resistivity system is based on the traditional
        
        
          four-electrode principle combined with automatic multiplexing
        
        
          for a larger number of electrodes (Damasceno et al., 2009). The
        
        
          system described here consists of: a constant current power
        
        
          source, a switching system and acquisition software. A 30V/2A
        
        
          programmable DC power supply type EL302P and MSL
        
        
          Datascan logger type 7220, both connected to a PC via RS 232
        
        
          interface, were used to measure the voltage and log the current
        
        
          by measuring the voltage drop across a 1 Ω high precision shunt
        
        
          resistor. A similar approach has been adopted in commercial
        
        
          equipment e.g. MPT/ERT 2004 system from Multi-Phase
        
        
          Technologies, LLC (MPT) (LaBrecque and Daily, 2008).
        
        
          Windows based data acquisition and control software named
        
        
          Resist has been developed to integrate the hardware and to
        
        
          control the data collection process. The user can set the current
        
        
          injected into the soil specimen and read the current, the voltage
        
        
          drop, and hence the resistance in a fully automatic procedure.
        
        
          To prevent electrode polarization (LaBrecque and Daily, 2008)
        
        
          short current pulses are used and an average reading (i.e.
        
        
          stacking) of a number of normal and reverse polarity readings
        
        
          are automatically acquired.
        
        
          The aim of the laboratory testing described here was to
        
        
          check the data quality of the developed system. A wide range of
        
        
          high precision reference resistors (ASTM G57, 2006) was used
        
        
          to calibrate the system, and the measurements were compared
        
        
          with those acquired with a Terrameter SAS 300C (ABEM)
        
        
          system. The results are reported in Table 1. It can be seen that
        
        
          Resist gives better results than the commercial Terrameter with
        
        
          a maximum error of 0.8%.
        
        
          Table 1. A comparison between Terrameter SAS 300C system and
        
        
          Resist reading for a range of reference resistors
        
        
          SAS 300 Terrameter
        
        
          Resist
        
        
          Reference
        
        
          Resistor
        
        
          (Ohm)
        
        
          Average
        
        
          Reading
        
        
          (Ohm)
        
        
          Percentage
        
        
          Error
        
        
          (%)
        
        
          Average
        
        
          reading
        
        
          (Ohm)
        
        
          Percentage
        
        
          Error
        
        
          (%)
        
        
          10
        
        
          9.9
        
        
          1.00
        
        
          10.0
        
        
          0.00
        
        
          56
        
        
          56.1
        
        
          0.18
        
        
          56.3
        
        
          0.54
        
        
          100
        
        
          98.0
        
        
          2.00
        
        
          99.2
        
        
          0.80
        
        
          120
        
        
          119.3
        
        
          0.58
        
        
          120.2
        
        
          0.17
        
        
          150
        
        
          149.0
        
        
          0.67
        
        
          150.1
        
        
          0.07
        
        
          220
        
        
          217.0
        
        
          1.36
        
        
          218.9
        
        
          0.50
        
        
          270
        
        
          268.0
        
        
          0.74
        
        
          270.5
        
        
          0.19
        
        
          370
        
        
          368.0
        
        
          0.54
        
        
          368.9
        
        
          0.30
        
        
          490
        
        
          486.0
        
        
          0.82
        
        
          489.0
        
        
          0.20
        
        
          590
        
        
          585.0
        
        
          0.85
        
        
          589.1
        
        
          0.15
        
        
          1000
        
        
          996.0
        
        
          0.40
        
        
          998.4
        
        
          0.16
        
        
          1120
        
        
          1118.0
        
        
          0.18
        
        
          1118.4
        
        
          0.14
        
        
          1220
        
        
          1217.0
        
        
          0.24
        
        
          1215.9
        
        
          0.33
        
        
          Figure 1. Resistivity-gravimetric water content relationship of a kaolin
        
        
          specimen
        
        
          Figure 2. Resistivity-water content relationships of BIONICS clay and
        
        
          different clays reported in the literature
        
        
          A resistivity box (ASTM G57, 2006) was constructed to
        
        
          measure resistivity of a Kaolin specimen during drying. A good
        
        
          comparison between Terrameter SAS 300C and Resist readings
        
        
          is shown in Figure 1 with a percentage difference less than
        
        
          1.59%.
        
        
          The developed system has been used to investigate drying
        
        
          and wetting of sandy clay sampled from the BIONICS project
        
        
          (Mendes, 2011). The soil is classified as being intermediate
        
        
          plasticity with Liquid  Limit  (43.3%),  Plastic  Limit (23.7%),
        
        
          Plasticity Index  of  19.6,  and  a  Liquidity  Index  of  -0.05. A
        
        
          resistivity probe based on a square arrangement (Habberjam and
        
        
          Watkins, 1967) with inter-electrode spacing of 15mm was
        
        
          constructed to monitor water content changes of a specimen
        
        
          subjected to controlled drying and wetting procedures. Figure 2
        
        
          shows the drying and wetting curve compared to different clays
        
        
          reported in the literature
        
        
          .
        
        
          The experimental data followed the power law function
        
        
          reported in the literature (Calamita et al. 2012), within the
        
        
          typical range of clay resistivity (1-100) Ohm.m (e.g. Loke
        
        
          2011). As resistivity is mainly controlled by water content, in
        
        
          both drying or wetting the resistivity is relatively low at high
        
        
          water content (the capillary and gravitational water ranges) and
        
        
          high at low water content (the range of adsorbed, lm, and lm-
        
        
          capillary water) (Pozdnyakov et al., 2006). However, the rate of
        
        
          the resistivity changes is higher at low water content due to air
        
        
          replacement of water in the pores. The well defined resistivity-
        
        
          water content relationship obtained in this study with high
        
        
          correlation coefficient 0.945 and 0.966 for drying and wetting
        
        
          respectively, suggest that it can be used to calibrate resistivity
        
        
          against water content (Muñoz-Castelblanc et al., 2011) and to
        
        
          estimate in situ water content changes (Calamita et al., 2012).